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Noori, Noor Sabah
- Preparation and Characterization of Novel Disubstituted 1,3- Oxazepinetetra- One from Schiff Bases Reaction with 3-Methylfuran-2,5-Dione and 3- Phenyldihydrofuran-2,5-Dione
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Authors
Affiliations
1 Pharmacy College, University Of Anbar, Anbar, IQ
2 Department of Ecology, College of Applied Sciences-Hit, University Of Anbar, Anbar, IQ
3 Department of Chemistry, College of Science, University Of Anbar, Anbar, IQ
1 Pharmacy College, University Of Anbar, Anbar, IQ
2 Department of Ecology, College of Applied Sciences-Hit, University Of Anbar, Anbar, IQ
3 Department of Chemistry, College of Science, University Of Anbar, Anbar, IQ
Source
Research Journal of Pharmacy and Technology, Vol 12, No 3 (2019), Pagination: 1008-1016Abstract
This research includes synthesis of new heterocyclic derivatives of novel disubstituted 1,3- oxazepine-tetra-one from Schiff bases reaction with 3-methylfuran-2,5-dione and 3-phenyldihydrofuran-2,5-dione. Schiff bases [A1- A5] were synthesized by the reaction of aromatic aldehydes with primary aromatic amines, in the presence of glacial acetic acid as catalyst in absolute ethanol. The novel derivatives[A6-A10] were obtained from treatment of Schiff bases with anhydrides. The synthesized compounds were identified by TLC and via spectral methods, their (FT-IR, 1H-NMR and 13C-NMR) and measurements of some of its physical properties.Keywords
1H-NMR, 13C-NMR, TLC, Schiff Bases, Oxazepine-Tetra-One.
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